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關注:1
2013-05-23 12:21
求翻譯:將(Ⅱ)(g, 0.1mol)充分溶解于THF中,用導針將溶液導入加有鎂屑(12g, 0.5mol)的燒瓶中,并用一顆碘粒引發格氏反應。滴液完畢后將水浴溫度調至THF回流并反應兩小時。反應完畢后將溶液導入另一燒瓶,滴加二甲基氯硅烷(ml, 0.15mol)。常溫攪拌過夜。反應加水終止。加入乙醚分液,水層繼續用乙醚洗滌,合并油層后用旋蒸蒸去溶劑,用正己烷作為展開劑過柱分離。蒸去展開劑,得Ⅲ( g, mol), 收率 %.是什么意思?![]() ![]() 將(Ⅱ)(g, 0.1mol)充分溶解于THF中,用導針將溶液導入加有鎂屑(12g, 0.5mol)的燒瓶中,并用一顆碘粒引發格氏反應。滴液完畢后將水浴溫度調至THF回流并反應兩小時。反應完畢后將溶液導入另一燒瓶,滴加二甲基氯硅烷(ml, 0.15mol)。常溫攪拌過夜。反應加水終止。加入乙醚分液,水層繼續用乙醚洗滌,合并油層后用旋蒸蒸去溶劑,用正己烷作為展開劑過柱分離。蒸去展開劑,得Ⅲ( g, mol), 收率 %.
問題補充: |
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2013-05-23 12:21:38
(Ⅱ) (g, 0.1mol) will be fully dissolved in thf solution to import the used needle plus magnesium shavings (12g, 0.5mol) in a flask, and an iodine tablets caused by the Grignard reaction. Drip completed after the water bath temperature raised to of thf reflux and response to two hours. The reaction i
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2013-05-23 12:23:18
Will (II) (g mol, 0.1 ) THF fully dissolved in the solution will be the guide pin import with chips (12 G, 0.5 mol) in a flask fitted with a iodine tablets that's caused reaction. After dripping the THEREAPY THF reflow temperature and reaction to two hours. After reaction solution will be imported i
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2013-05-23 12:24:58
(Ⅱ) (g, 0.1mol) the full dissolution in THF, inducts with the guide stem the solution Canada has the magnesium filings (12g, 0.5mol) in the flask, and responded with idodine grain of initiation standard.After the dropping liquid finished transfers to the water bath temperature the THF backflow and r
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2013-05-23 12:26:38
(Ii) (g, 0.1mol) fully dissolved in THF, with guide pin import solution adding magnesium scrap (12g, 0.5mol) in flasks, and use a Grignard reaction with iodine tablets thrown. Liquid after the bath water temperature drops to THF return and response for two hours. Reactions after the solution import
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2013-05-23 12:28:18
正在翻譯,請等待...
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